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https://hdl.handle.net/2440/4396
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Type: | Journal article |
Title: | Preparation and characterisation of the dicarbon cluster complex Ru5(m5-C2)(m-SMe)2(m-PBu2)2(CO)11 |
Author: | Bruce, M. Adams, C. |
Citation: | Australian Journal of Chemistry: an international journal for chemical science, 1996; 49(4):517-520 |
Publisher: | CSIRO Publishing |
Issue Date: | 1996 |
ISSN: | 0004-9425 |
Abstract: | <jats:p>The preparation of the bis -tertiary phosphine C2(Pbu2)2 ( dpba ) is described. Pyrolysis of the ruthenium carbonyl derivative {Ru3(CO)11}2(μ- dbpa ) gives Ru5(μ5-C2PBu2)(μ-PBu2)(CO)13[in 41% overall yield from Ru3(CO)12)] which in turn reacts with Me2S2 to give Ru5(μ5-C2)(μ5-SMe)2(μ-PBu2)2(CO)11(19%). </jats:p> |
DOI: | 10.1071/CH9960517 |
Published version: | http://dx.doi.org/10.1071/ch9960517 |
Appears in Collections: | Aurora harvest 6 Chemistry publications |
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