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https://hdl.handle.net/2440/74391
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Type: | Journal article |
Title: | 1,4-Di-tert-butyl (2R,3R)-2-({(2E)-3-[4(acetyloxy)phenyl]prop-2-enoyl}oxy)-3hydroxybutanedioate |
Author: | Hixson, J. Taylor, D. Ng, S. Tiekink, E. |
Citation: | Acta Crystallographica Section E: Structure Reports Online, 2012; 68(2):O509-O521 |
Publisher: | Blackwell Munksgaard |
Issue Date: | 2012 |
ISSN: | 1600-5368 1600-5368 |
Statement of Responsibility: | Josh L. Hixson, Dennis K. Taylor, Seik Weng Ng and Edward R. T. Tiekink |
Abstract: | The title compound, C₂₃H3₃₀O₉, has an approximate T-shape with the tert-butyl ester groups lying either side of the benzene ring. The acetyl group is almost perpendicular to the benzene ring to which it is connected [C-C-O-C torsion angle = -106.7 (3)°]. The conformation about the C=C double bond [1.331 (4) Å] is E. Linear supramolecular chains along the a axis mediated by hydroxy-carbonyl O-H...O hydrogen bonds feature in the crystal packing. The same H atom is also involved in an intramolecular O-H...O interaction. |
Rights: | Copyright © International Union of Crystallography |
DOI: | 10.1107/S160053681200236X |
Published version: | http://dx.doi.org/10.1107/s160053681200236x |
Appears in Collections: | Aurora harvest 4 Wine Science publications |
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